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Function investigation of stone mastic asphalt (SMA) mixture partly containing basic oxygen furnace (BOF) slag

Abstract

Aims

In this paper, the effect of the size gradations of basic oxygen furnace (BOF) slag on the functional performances of stone mastic asphalt (SMA) mixture including skid and deformation resistances was investigated.

Methods

The industrially produced BOF slag coarse aggregates (BSCA) with size gradations of 4.75-9.5 mm and 9.5-16 mm were used. SMA mixtures were designed according to Marshall procedure. British pendulum number (BPN), indicating the skid resistance of asphalt mixture, was measured by a British pendulum skid resistance device. Flow number (FN) and Marshall quotient (MQ), reflecting the deformation resistance of asphalt mixture, were determined, respectively, based on the results of dynamic creep test and Marshall test (stability and flow value).

Results

Showed that BSCA with a size gradation of 9.5-16 mm performed better in improving the skid and deformation resistance of SMA mixture than BSCA with a size gradation of 4.75-9.5 mm. Furthermore, BSCA with combined size gradations, namely, 4.75-16 mm, worked the best.

Conclusions

These conclusions would benefit the future extensive utilization of BSCA in asphalt pavement.

J Appl Biomater Funct Mater 2016; 14(Suppl. 1): e68 - e72

Article Type: ORIGINAL RESEARCH ARTICLE

DOI:10.5301/jabfm.5000307

OPEN ACCESS ARTICLE

Authors

Zongwu Chen, Shaopeng Wu, Ling Pang, Jun Xie

Article History

Disclosures

Financial support: This work was financially supported by the National Key Scientific Apparatus Development Program (No. 2013YQ160501), the International Science & Technology Cooperation Program of China (No. 2013DFE83100), the 973 Program (No. 2014CB932104) and the Fundamental Research Funds for the Central Universities (No. 2016-YB-002).
Conflict of interest: None of the authors has financial interest related to this study to disclose.

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Introduction

Asphalt pavement is widely utilized in the pavement construction due to its driving comfort and good pavement performances. Environmental protection, functional application and resource conservation are the major concerns in the construction of future asphalt pavements (1-2-3). For instance, the shortage of natural resources has accelerated the utilization of secondary materials (3-4-5-6-7-8-9-10), among which, the recycling basic oxygen furnace (BOF) slag is a typical representative (4-5-6-7-8-9-10).

BOF slag is a by-product generated during the process of steelmaking, which accounts for 13% of the raw steel output (9), and can be applied in many fields like purification engineering and road construction. The use of BOF slag in road construction is quite promising due to the high efficiency. Many previous researches indicated that BOF slag can improve certain properties of asphalt mixture (4-5-6-7-8-9-10). Chen et al reported that, compared to basalt and granite, BOF slag showed better bonding performance with asphalt binder (4), and BOF slag coarse aggregate (BSCA) can improve the fatigue crack resistance of dense asphalt mixture (8). Xie et al stated that asphalt mixture containing BSCA obtained satisfactory moisture resistance (7). After evaluating the effect of different BSCA substitution dosages on the performance of porous asphalt mixture, Shen et al recommended 100% BSCA as a coarse aggregate substitution (9). In these studies, the BSCA with particle size ranging from 4.75 mm to the maximum size restricted by the designed gradation was usually used. However, the effect of particle size on the performances of asphalt mixture has not been well investigated. The coarse part in a hybrid gradation used in entity engineering is usually the combination of several coarse aggregates with different size gradations. Therefore, it is meaningful to evaluate the effect of BSCA’s size gradations on the pavement performances of asphalt mixture in order to realize the multilevel utilization of BSCA.

Stone mastic asphalt (SMA) mixture is a gap-graded hot mix asphalt mixture that belongs to functional pavement materials. It mainly consists of coarse aggregates and high content of asphalt mortar (11). The high proportion of coarse aggregates provides great texture depths and a stable skeleton through stone-to-stone contact (12), which benefits the skid and deformation resistances of SMA pavement. As performance indexes of asphalt pavement, skid and deformation resistances are two important properties (12-13-14-15). Wu et al evaluated the feasibility of recycling BSCA in SMA mixtures (13), and SMA mixture with 100% BSCA as a substitution of basalt coarse aggregate was identified to possess 15% higher dynamic stability in the laboratory environment. They kept recording the pavement performances of the test section paved with BSCA for two years, and results showed that the British pendulum number (BPN) of test section merely reduced by 11% during the service period from 6 to 24 months.

In this research, the effect of BSCA’s size gradation on the skid and deformation resistances of SMA mixture was investigated. BPN value, an indicator of asphalt mixture’s skid resistance, was measured according to ASTM E303 (16). Marshall quotient (MQ) and flow number (FN), two indicators of asphalt mixture’s deformation resistance, were determined based on the test results of Marshall stability and flow value (ASTM D6927) (17), and dynamic creep test (BS EN 12697-25) (18), respectively. Basalt SMA mixture functioned as a control group.

Experimental procedure

Raw materials

Two types of coarse aggregates, namely, BSCA and basalt (both with size gradations of 4.75-9.5 mm and 9.5-16 mm), were used. Meanwhile, basalt was also applied as fine aggregate. Two BSCA production lines were built in Hubei, China. One was utilized to produce BSCA with size gradations of 9.5-19 mm and 19-31.5 mm, while the other one was designed for the production of BSCA with size gradations of 4.75-9.5 mm and 9.5-16 mm. BSCA received sufficient aging treatment to remove the free lime and easily fractured parts like honeycomb particles contained in slags. The basic physical properties of the aggregates were tested according to Chinese standard (19), and results were shown in Table I. Besides, SBS modified asphalt binder with penetration of 58.5 (0.1 mm at 25°C), ductility beyond 20.0 cm (5 cm/min, 5°C), and softening point of 61.5°C, limestone powder and polyester fiber were used. The basic physical properties of all raw materials satisfied the requirements of Chinese specification (20).

The basic physical properties of aggregates

Parameter measured Coarse Fine Criteria in China
BSCA Basalt Basalt
BSCA = basic oxygen furnace slag coarse aggregate.
Size range (mm) 9.5-16 4.75-9.5 9.5-16 4.75-9.5 0-4.75
Apparent SG 3.411 3.474 2.782 2.788 2.769 ≥2.5
Water absorption (%) 1.5 1.7 0.7 0.8 1.1 ≤3
Flakiness and elongation (%) 6.3 10.2 9.2 13.4 NA ≤18
LA abrasion (%) 14.3 14.3 18.1 18.1 NA ≤28
Fine aggregate angularity (%) NA NA NA NA 48 ≥30
Sand equivalent (%) NA NA NA NA 64 ≥60

Design of SMA mixtures

SMA mixtures with nominal maximum size of 13.2 mm were designed in this research, and the compositions of each mixture were shown in Table II. A volume control method was used in order to maintain constant volume composition of different SMA mixtures. Aggregates with size gradations of 9.5-16 mm, 4.75-9.5 mm and below 4.75 mm accounted for 45%, 29% and 16% of the total volume of the mineral mixture, respectively. Limestone filler occupied 10% of the total volume of the mineral mixture. In order to obtain satisfied hybrid gradations of mineral mixtures, the proportions of BSCA with different size gradations (9.5-16 mm, 4.75-9.5 mm) were not the same due to specific particle size distribution for each type of BSCA. It also suggested that the mix proportions for different types of BSCA cannot change arbitrarily when the design type of asphalt mixture was determined. The mix proportions used in this research can be copied in the construction of future BOF slag SMA pavement. Therefore, the focus of this research was on the size gradations, not on the proportions of different types of BSCA.

The compositions and volumetric properties of different SMA mixtures

Mixture types 9.5-16 mm 4.75-9.5 mm 0-4.75 mm Filler OAC (%) VMA (%) VFA (%)
OAC = optimum asphalt content; BSCA = basic oxygen furnace slag coarse aggregate; SMA = stone mastic asphalt; VMA = voids in mineral aggregate; VFA = voids filled with asphalt.
S1 45% BSCA 29% BSCA 16% basalt 10% limestone 6.20 18.6 78.7
S2 45% BSCA 29% basalt 16% basalt 10% limestone 6.15 18.7 78.1
S3 45% basalt 29% BSCA 16% basalt 10% limestone 6.10 18.2 78.0
S4 45% basalt 29% basalt 16% basalt 10% limestone 6.00 17.9 77.7
Requirements ≥17.0 75-85

The optimum asphalt content (OAC) was determined using steps as follows: (1) Based on the common range of asphalt contents for SMA mixtures, five asphalt contents (5.4%, 5.7%, 6.0%, 6.3%, and 6.6%) were considered for each SMA mixture; (2) then, each SMA mineral mixture was mixed with these five asphalt contents, respectively; (3) finally, standard Marshall test was carried out for the mixed SMA specimens (21). Afterwards, whether the volumetric parameters of SMA mixture with OAC were qualified or not were examined. The detailed information of each SMA mixture were shown in Table II, where the volumetric parameters met the requirements of Chinese specification (20).

Skid and deformation resistances of SMA mixtures

The slab specimens with a length of 300 mm, a width of 300 mm and a height of 50 mm were prepared for the antiskid test. The BPN values of slab specimens were determined at both dry and wet conditions using the British pendulum tester, shown in Figure 1A. The test process was performed following ASTM E303 (16). The surface of slab specimens ready for the test should be clean and free of loose particles. Four repeated tests were conducted for each specimen under dry and wet conditions, respectively.

Test setup: (A) is for British pendulum number (BPN) test, (B) and (C) are for dynamic creep test.

The Marshall test (stability and flow value) was conducted according to ASTM D6927 (17). Marshall specimens with a height of 63.5 mm and a diameter of 101.6 mm were prepared by using a standard Marshall hammer. Four specimens for each SMA mixture were prepared, and all specimens were immersed in 60oC water bath for 30-40 min. A HM-3000 master loader with a constant deformation rate of 50 mm/min was used to test the Marshall specimens.

The dynamic creep test was conducted according to BS EN 12697-25 (18), and modification has been made on the dimension of cylindrical specimens. Specimens with a diameter of 100 mm and a height of 100 mm were cored from double-layer slab compacted by the roller as shown in Figure 1B. Creep test was conducted by UTM-25 as shown in Figure 1C (3), where the applied stress was 0.1 MPa, and the haversine load pulse consisted of a 0.1 s loading period and a 0.9 s rest period. Besides, the test temperature was fixed at 60oC, and four repeated tests for each SMA mixture were conducted.

Results and discussions

Effect of BSCA’s size gradation on the skid resistance

The BPN values of SMA mixtures under both dry and wet conditions were shown in Figure 2. It can be seen that under dry conditions, BSCA with a size gradation of 9.5-16 mm, 4.75-9.5 mm displayed higher BPN values by 6.3% and 3.4%, respectively, compared to the pure basalt. Moreover, BSCA with the combination of these two size gradations, namely, 4.75-16 mm, performed even better than the previously separated BSCA components. However, the increment of BPN value caused by the combination was not the simple sum of the increments caused by their separated components. Under wet condition, similar effect was observed. In comparison to basalt SMA mixture, BSCA with a size gradation of 4.75-9.5 mm, 9.5-16 mm and 4.75-16 mm showed increased BPN values by 2.4%, 4.8% and 9.1%, respectively. Therefore, BSCA played a positive role in enhancing the skid resistance of SMA mixture. This effect was more apparent to coarser BSCA. The combination of BSCA with the two size gradations demonstrated the best skid resistance among all these SMA mixtures.

British pendulum number (BPN) values of different stone mastic asphalt (SMA) mixtures.

Effect of BSCA’s size gradation on the deformation resistance

The MQ, the ratio of Marshall stability to flow value, was used as an indicator to reflect the creep deformation resistance of asphalt mixture (22). The Marshall stability and MQ of SMA mixtures were shown in Figure 3. It showed that the BSCA with a size gradation of 4.75-9.5 mm, 9.5-16 mm and 4.75-16 mm increased the Marshall stability of SMA mixtures by 4.2%, 3.3% and 8.3%, respectively. The high alkalinity of BSCA, which was of benefit for the adhesion between steel slag and asphalt binder, may have contributed to it. Both the two types of BSCA (9.5-16 mm and 4.75-9.5 mm) displayed increased MQ, and the increase of MQ caused by the former was about 1.4 times higher than the latter. A larger MQ indicated a higher stiffness, so that the asphalt mixture had a greater ability to spread the applied load and resist creep deformation (23). Therefore, BSCA with a size gradation of 9.5-16 mm played a more significant role in improving the deformation resistance of SMA mixture. Similarly, SMA mixture containing BSCA with the combined size gradations performed the best among all SMA mixtures.

Marshall stability and Marshall quotient of different stone mastic asphalt (SMA) mixtures.

The dynamic creep deformation curve consists of three stages as shown in Figure 4 (3). In the first stage, the strain growth rate rapidly decreases until reaching a constant value, which indicates the start of the secondary stage. The secondary stage lasts for a very long period, and stable increase of total strain can be observed in this stage. However, the situation can be quite different when referring to the third stage. The strain growth rate rapidly increases and the total strain becomes very high in a short time, which finally results in failure. Load repeated cycles recorded at the start point of the third stage is known as the flow number (FN), which reflects the deformation resistance limit of asphalt mixture.

Three stages of dynamic creep deformation curve.

The FN of each SMA mixture was shown in Figure 5. It can be seen that SMA mixtures containing BSCA obtained larger FN than pure basalt SMA mixture. BSCA with a size gradation of 9.5-16 mm also showed more positive effect on increasing FN than BSCA with a size gradation of 4.75-9.5 mm, and the increase caused by BSCA with a size gradation of 9.5-16 mm was 2.4 times larger. Compared to BSCA with a size gradation of 9.5-16 mm, the superiority of BSCA with combined size gradations was small. It further proved that the effect of coarser BSCA on enhancing the deformation resistance of SMA mixture was much more significant. This may be related to the stable skeleton consisting of coarser particles.

Flow numbers of different stone mastic asphalt (SMA) mixtures.

Conclusions

The primary objective of this research was to evaluate the skid and deformation resistances of SMA mixtures containing BSCA with different size gradations. BSCA with size gradations of 9.5-16 mm, 4.75-9.5 mm accounted for 45%, 29% of the total volume of the mineral mixture, respectively. The following conclusions are obtained:

BSCA with a size gradation of 4.75-9.5 mm, 9.5-16 mm, and 4.75-16 mm increased the BPN value of SMA mixture by 3.4%, 6.3% and 11.4%, respectively, under dry condition, and 2.4%, 4.8% and 9.1%, respectively, under wet condition. This finding indicated that BSCA with coarser particles was more effective in improving the antiskid function of SMA mixture. Moreover, results showed that BSCA with the combined size gradations performed the best.

Compared to pure basalt SMA mixture, SMA mixtures containing BSCA with a size gradation of 4.75-9.5 mm, 9.5-16 mm, and 4.75-16 mm, showed higher MQ by about 8.7%, 20.8%, and 29.8%, respectively, with an increase in flow number (FN) as 4.6%, 15.5%, and 16.3%, respectively. These results illustrated that BSCA with coarser particles also performed better in improving the deformation resistance of SMA mixture. Furthermore, BSCA with the combined size gradations was again proved to be the most effective among all mixtures.

Disclosures

Financial support: This work was financially supported by the National Key Scientific Apparatus Development Program (No. 2013YQ160501), the International Science & Technology Cooperation Program of China (No. 2013DFE83100), the 973 Program (No. 2014CB932104) and the Fundamental Research Funds for the Central Universities (No. 2016-YB-002).
Conflict of interest: None of the authors has financial interest related to this study to disclose.
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Authors

Affiliations

  • State Key Laboratory of Silicate Materials for Architectures, Wuhan University of Technology, Wuhan - China

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